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age and hay, potatoes, safflower seed, salts (alkanolamine salts, ammonium soybeans, soybean forage and hay, and salt, or sodium salt) in or on raw agrisugar beet roots and tops at 0.05 part cultural commodities as follows: per million.

1 part per million in or on soybean

forage and hay. § 180.278 Phenmedipham; tolerances for

0.1 part per million (negligible resiresidues.

due) in or on alfalfa; alfalfa hay; alTolerances are established for negli- monds; almond hulls; apples; apricots; gible residues of the herbicide phen- barley (grain, forage and straw); medipham (methyl m-hydroxycarbani- beans; bean forage and hay; birdsfoot late m-methylcarbanilate) in or on raw trefoil and trefoil hay; blackberries; agricultural commodities as follows: blueberries; boysenberries; cherries;

0.2 part per million in or on beets. citrus; clover and clover hay; corn

0.1 part per million in or on sugar fodder and forage; corn grain includbeet roots and tops.

ing popcorn; fresh corn including (37 FR 14302, June 19, 1972)

sweet corn (kernels plus cob with husk

removed); cotton forage; cottonseed; $ 180.279 3-(4-Bromo-3-chlorophenyl)-1. cottonseed hulls; cucurbits; currants;

methoxy-1-methylurea; tolerances for dates; figs; filberts; garlic; gooseberresidues.

ries; grapes; hops; loganberries; nectarTolerances are established for com

ines; oats (grain, forage, and straw); bined residues of the herbicide 3-(4

olives; onions; peaches; peanuts; bromo-3-chlorophenyl)-1-methoxy-1.

peanut forage, hay, and hulls; pears; methylurea and its metabolites con

peas; pea forage and hay; pecans; taining the 4-bromo-3-chloroaniline

plums (prunes); potatoes; raspberries; moiety in or on raw agricultural com

rye (grain, forage, and straw); soymodities as follows:

beans; strawberries; vetch and vetch

hay; walnuts; and wheat 0.2 part per million (negligible resi

(grain, due) in or on corn fodder and forage,

forage, and straw). corn grain, fresh corn including sweet (39 FR 43290, Dec. 12, 1974) corn (kernels plus cob with husk removed), potatoes, soybean forage, soy- § 180.282 2-Chloro-N,N-diallylacetamide; beans, wheat grain, and wheat straw.

tolerances for residues. 0.1 part per million (negligible resi

Tolerances are established for neglidue) in meat, fat, and meat byproducts

gible residues of the herbicide 2of cattle, goats, hogs, horses, poultry,

chloro-N,N-diallylacetamide in or on and sheep.

the raw agricultural commodities cab(37 FR 334, Jan. 11, 1972, as amended at 37 bage, castor beans, celery, corn grain FR 23335, Nov. 2, 1972)

(includes popcorn), fresh corn includ

ing sweet corn (kernels plus cobs with $ 180.280 Dimethyl phosphate of a-methyl- husk removed), corn forage or fodder benzyl 3-hydroxy-cis-crotonate; toler

(including sweet corn, field corn, and ances for residues.

popcorn), dried beans, lima beans, lima Tolerances are established for negli

bean forage, onions, peas, pea forage, gible residues of the insecticide di- potatoes, snap beans, snap bean methyl phosphate of a-methylbenzyl forage, sorghum

grain,

sorghum 3-hydroxy-cis-crotonate in meat, fat, forage, soybeans, soybean forage, sugand meat byproducts of cattle, goats, arcane, sweetpotatoes, and tomatoes hogs, and sheep and in milk at 0.02 at 0.05 part per million. part per million.

$ 180.283 2, 3, 6-Trichlorophenylacetic $ 180.281 Dinoseb; tolerances for residues. acid; tolerances for residues.

Tolerances are established for resi- A tolerance of 0.1 part per million is dues of the herbicide, insecticide, and established for negligible residues of fungicide dinoseb (2-sec-butyl-4,6-dini- the herbicide 2,

6trophenol) from application of its trichlorophenylacetic acid in or on phenol or its readily hydrolyzable sugarcane,

such residues resulting

3,

from application of its dimethylamine or sodium salts.

$ 180.287 (Reserved)

$ 180.287 2 - (Thiocyanomethylthio) ben

zothiazole; tolerances for residues.

§ 180.284 Zinc phosphide; tolerances for

residues. Tolerances are established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on raw agricultural commodities as follows:

0.1 part per million in or on grasses (rangeland).

0.01 part per million in or on grapes and sugarcane. (40 FR 31237, July 25, 1975, as amended at 40 FR 55857, Dec. 2, 1975)

corn

anc

Tolerances are established for negli gible residues of the fungicide 2-(thio cyanomethylthio) benzothiazole in or on barley (fodder, forage, grain, ang straw),

(fodder, forage, grain), cotton forage, cottonseed, oats (fodder, forage, grain, and straw), rice (grain and straw) safflower (fodder. forage, and seed), sorghum (fodder, forage, and grain), sugarbeets (root and tops), and wheat (fodder, forage, grain, and straw) at 0.1 part per mil lion.

[40 FR 33453, Aug. 8, 1975)

$ 180.285 Chlordimeform; tolerances for

residues. Tolerances are established for combined residues of the insecticide chlordimeform (N'-(4-chloro-o-tolyl)-N,N-dimethylformamidine) and its metabolites containing the 4-chloro-o-toluidine moiety (calculated as the insecticide) from application of the insecticide as the free base or as the hydrochloride salt in or on raw agricultural commodities as follows:

12 parts per million in or on pears.

5 parts per million in or on cottonseed, cherries, nectarines, and peaches.

4 parts per million in or on plums (fresh prunes).

3 parts per million in or on apples.

2 parts per million in or on broccoli, brussels sprouts, cabbage, and cauliflower.

1 part per million in or on tomatoes.

0.25 part per million in meat, fat, and meat byproducts of cattle, goats, hogs, horses, poultry, and sheep.

0.05 part per million in eggs and milk.

0.1 part per million in or on walnuts. [37 FR 9483, May 11, 1972, as amended at 38 FR 24, Jan. 3, 1973; 39 FR 7930, Mar. 1, 1974; 39 FR 26155, July 17, 1974)

$ 180.289 Methanearsonic acid; tolerance

for residues. Tolerances are established for resi dues of the herbicide methanearsonic acid (calculated as As,0z) from appli cation of the disodium and monoso dium salts of methanearsonic acid ir or on raw agricultural commodities a follows:

0.7 part per million in or on cotton seed.

0.35 part per million in or on citrus fruit.

[37 FR 7158, Apr. 11, 1972)

§ 180.290 Fluorodifen; tolerances for resi

dues. Tolerances are established for com bined residues of the herbicide fluoro difen (p-nitrophenyl-2-nitro-4-(tri fluoromethyl) phenylether) and its metabolites p-nitrophenyl-2-amino-4. (trifluoromethyl) phenylether and pnitrophenol in or on raw agricultura. commodities as follows:

0.2 part per million (negligible residue) in or on peanut hulls, peanuts. and peanut vine hay.

0.1 part per million (negligible residue) in or on soybean forage, soybeans, and seed and pod vegetables and their forages.

§ 180.286 1-Chloro-2-nitropropane; toler

ances for residues. A tolerance of 0.05 part per million is established for negligible residues of the fungicide 1-chloro-2-nitropropane and its metabolite 2-nitropropanol (calculated as 1-chloro-2-nitropropane) in or on the raw agricultural commodities cottonseed and melons.

(37 FR 16494, Aug. 15, 1972)

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Parts per Commodity

million Lemons

2 Lettuce

5 Mint, hay

2 Nectarines.

5 Oranges.

2 Peaches

5 Peanuts

0.1(N) Peanuts, hulls

0.1(N) Peas.....

5 Peas, vines

10 Pomegranates

0.2(N) Sorghum, forage.

1 Sorghum, grain.

0.2(N) Soybeans..

0.2(N) Soybeans, forage

10 Spinach

6 Tangerines...

2 Vegetables, leafy (exc broccoli, brussels

sprouts, cabbage, cauliflower, celery,

endive (escarole), lettuce, and spinach) 0.2(N) Vegetables, fruiting

0.2(N) Vegetables, root crop

0.2(N) (41 FR 2822, Jan. 20, 1976, as amended at 43 FR 25121, June 9, 1978)

beet tops (of which no more than 1 part per million is carbamates).

1 part per million in or on peppers and in or on rice straw (of which no more than 0.2 part per million is carbamates).

0.5 part per million in or on strawberries (of which no more than 0.2 part per million is carbamates).

0.2 part per million in or on corn grain, including popcorn (of which no more than 0.1 part per million is carbamates), in or on peanuts (of which no more than 0.1 part per million is carbamates), and in or on rice.

0.1 part per million in milk (of which no more than 0.02 part per million is carbamates).

0.1 part per million in or on bananas, coffee beans, sorghum grain, sugar beets, and sugarcane.

0.05 part per million in the fat, meat, and meat by-products of cattle, goats, hogs, horses, and sheep (of which no more than 0.02 part per million is carbamates). (39 FR 20597, June 12, 1974, as amended at 40 FR 4657, Jan. 31, 1975; 40 FR 13500, Mar. 27, 1975; 41 FR 763, Jan. 5, 1976)

$ 180.254 Carbofuran; tolerances for resi.

dues. Tolerances are established for combined residues of the insecticide carbofuran (2,3-dihydro-2,2-dimethyl-benzsofuranyl-N-methylcarbamate), its carbamate metabolite 2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benzofuranyl-Nmethylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7benzofuranol, 2,3-dihydro-2,2-dimethyl-3-oxo-7-benzofuranol, and 2,3dihydro-2, 2-dimethyl-3, 7-benzofurandiol in or on the following raw agricultural commodities:

40 parts per million in or on alfalfa hay (of which no more than 20 parts per million are carbamiates).

25 parts per million in or on corn fodder and forage (of which no more than 5 parts per million are carbamates).

10 parts per million in or on alfalfa (fresh) (of which no more than 5 parts per million are carbamates).

5 parts per million in or on peanut hulls (of which no more than 1 part per million is carbamates).

3 parts per million in or on sorghum fodder and forage (of which no more than 0.5 part per million is carbamates).

2 parts per million in or on potatoes (of which no more than 1 part per million is carbamates) and in or on sugar

§ 180.255 m-(1-Methylbutyl) phenyl meth

ylcarbamate and m-(1-ethylpropyl) phenyl methylcarbamate; tolerances

for residues. Tolerances are established for negligible residues of an insecticide that is a mixture consisting of 75 percent m(1-methylbutyl) phenyl methylcarbamate and 25 percent m-(l-ethylpropyl) phenyl methylcarbamate in or on the raw agricultural commodities corn grain, fresh corn including sweet corn (kernels plus cob with husk removed), corn fodder and forage, rice, and rice straw at 0.05 part per million (such tolerances to cover residues of both components).

(37 FR 6848, Apr. 5, 1972)

$ 180.256 p-Chlorophenyl-2,4,5-trichloro

phenyl sulfide; tolerances for residues.

A tolerance of 0.1 part per million is established for negligible residues of the insecticide p-chlorophenyl-2,4,5trichlorophenyl sulfide in or on the raw agricultural commodity apples.

$ 180.257 Chloroneb; tolerances for resi.

dues. Tolerances are established for residues of the fungicide chloroneb (1,4dichloro-2,5-dimethoxybenzene) and its metabolite 2,5-dichloro-4-methoxy. phenol (calculated as chloroneb) in or on raw agricultural commodities as follows:

2 parts per million in or on cotton forage and vines (forage) of beans and soybeans.

0.2 part per million in meat, fat, and meat byproducts of cattle, goats, hogs, horses, and sheep.

0.1 part per million (negligible resi. due) in or on beans, cottonseed, soybeans, and sugarbeets (roots and tops).

0.05 part per million (negligible residue) in milk.

Parts per
million

0.1
0.1
0.1
10
10
0.1
0.1
10
0.1
3
0.1
0.1
0.1
5
10
0.1
0.1
0.1
15
0.1
0.1
0.1

Commodity Cattle, fat.. Cattle, mbyp Cattle, meat. Corn, fodder Corn, forage. Corn, grain.. Cottonseed. Cranberries. Eggs.... Figs.. Goats, fat Goats, mbyp Goats, meat Grapefruit Grapes ... Hogs, fat... Hogs, mbyp. Hogs, meat Hops.. Horses, fat.. Horses, mbyp. Horses, meat. Lemons. Milk, fat (0.08 ppm in milk). Mint Nectarines Oranges. Peaches.. Peanuts.. Peanuts, forage Peanuts, hay Peanuts, hulls Pears Plums (fresh prunes). Poultry, fat Poultry, mbyp Poultry, meat Potatoes Sheep, fat.... Sheep, mbyp. Sheep, meat. Sorghum, fodder. Sorghum, forage Sorghum, grain Strawberries Walnuts...... (41 FR 25001, June 22, 1976)

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§ 180.258 2-(ethylamino)-4-(isopropyl

amino)-6-(methylthio)-s-(triazine); to

lerances for residues. Tolerances are established for residues of the desiccant and herbicide 2(ethylamino)-4-(isoproprylamino)-6(methylthio)-s-(triazine) in or on raw agricultural commodities as follows:

0.5 part per million in or on corn fodder and forage.

0.25 part per million in or on bananas, corn grain, fresh corn including sweet corn (kernels plus cob with husk removed), pineapples, pineapple fodder and forage, potatoes, sugarcane, and sugarcane fodder and forage.

0.1 part per million (negligible residue) in or on grapefruit and oranges. (36 FR 22540, Nov. 25, 1971, as amended at 38 FR 7330, Mar. 20, 1973)

3 7 0.1 0.1 0.1 0.1 0.1 0.1 0.1 10 10 10 7 0.1

§ 180.259 Propargite; tolerances for resi

dues. Tolerances are established for residues of the pesticide propargite (2- (ptert-butylphenoxy) cyclohexyl 2-propynyl sulfite) in or on the following raw agricultural commodities.

§ 180.260 Norea; tolerances for residues.

Tolerances are established for negligible residues of the herbicide norea (3-(hexahydro-4,7-methanoindan-5-yl)1,1-dimethyl urea) in or on the raw agricultural commodities cottonseed, potatoes, sorghum (cane, forage, and grain), soybeans, spinach, and sugarcane at 0.2 part per million. § 180.261 N-(Mercaptomethyl)phthalimide

SIO, O-dimethyl phosphorodithioate) and its oxygen analog; tolerances for

residues. Tolerances are established for the cholinesterase-inhibiting residues of the insecticide N-(mercaptomethyl) phthalimide S(0,0-dimethyl phos

Commodity
Almonds
Almonds, hulls
Apples.
Apricots..
Beans, dry.
Beans, succulent

Parts per
million

0.1 55 3 7 0.2 20

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