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§ 261.32 Hazardous wastes from specific sources.

The following solid wastes are listed hazardous wastes from specific sources unless they are excluded under §§ 260.20 and 260.22 and listed in appendix IX.

Industry and EPA hazardous waste No.

Wood preservation: K001

Inorganic pigments:

K002

K003

K004

K005

K006

K007

K008

Organic chemicals:

K009

K010

K011

K013

K014

K015

K016

K017

K018

K019

K020

K021

K022

K023

K024

K025

K026

K027

K028

K029

K030

K083

K085

K093

K094

K095

K096

K103

K104

K105

K107

K108

K109

K110

K111

K112

K113

K114

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Bottom sediment sludge from the treatment of wastewaters from wood preserving (T) processes that use creosote and/or pentachlorophenol.

Wastewater treatment sludge from the production of chrome yellow and orange (T)
pigments.

Wastewater treatment sludge from the production of molybdate orange pigments
Wastewater treatment sludge from the production of zinc yellow pigments....
Wastewater treatment sludge from the production of chrome green pigments
Wastewater treatment sludge from the production of chrome oxide green pigments
(anhydrous and hydrated).

Wastewater treatment sludge from the production of iron blue pigments
Oven residue from the production of chrome oxide green pigments...

Distillation bottoms from the production of acetaldehyde from ethylene
Distillation side cuts from the production of acetaldehyde from ethylene...
Bottom stream from the wastewater stripper in the production of acrylonitrile.
Bottom stream from the acetonitrile column in the production of acrylonitrile.
Bottoms from the acetonitrile purification column in the production of acrylonitrile
Still bottoms from the distillation of benzyl chloride

Heavy ends or distillation residues from the production of carbon tetrachloride.
Heavy ends (still bottoms) from the purification column in the production of
epichlorohydrin.

Heavy ends from the fractionation column in ethyl chloride production.....

(R, T)

Heavy ends from the distillation of ethylene dichloride in ethylene dichloride (T) production.

Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer (T) production.

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Aqueous spent antimony catalyst waste from fluoromethanes production.
Distillation bottom tars from the production of phenol/acetone from cumene..
Distillation light ends from the production of phthalic anhydride from naphthalene
Distillation bottoms from the production of phthalic anhydride from naphthalene.
Distillation bottoms from the production of nitrobenzene by the nitration of benzene.
Stripping still tails from the production of methy ethyl pyridines
Centrifuge and distillation residues from toluene diisocyanate production..
Spent catalyst from the hydrochlorinator reactor in the production of 1,1,1-trichlor- (T)
oethane.

Waste from the product steam stripper in the production of 1,1,1-trichloroethane.

(R, T)

Column bottoms or heavy ends from the combined production of trichloroethylene (T) and perchloroethylene.

Distillation bottoms from aniline production

Distillation or fractionation column bottoms from the production of chlorobenzenes.
Distillation light ends from the production of phthalic anhydride from ortho-xylene..
Distillation bottoms from the production of phthalic anhydride from ortho-xylene.
Distillation bottoms from the production of 1,1,1-trichloroethane.

Heavy ends from the heavy ends column from the production of 1,1,1-trichloroeth

ane.

Process residues from aniline extraction from the production of aniline...
Combined wastewater streams generated from nitrobenzene/aniline production

Separated aqueous stream from the reactor product washing step in the production (T)
of chlorobenzenes.

Column bottoms from product separation from the production of 1,1-dimethyl- (C,T)
hydrazine (UDMH) from carboxylic acid hydrazines

Condensed column overheads from product separation and condensed reactor vent (I,T)
gases from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid
hydrazides
Spent filter cartridges from product purification from the production of 1,1-dimethylhy- (T)
drazine (UDMH) from carboxylic acid hydrazides

Condensed column overheads from intermediate separation from the production of (T)
1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

(C,T)

Product washwaters from the production of dinitrotoluene via nitration of toluene... Reaction by-product water from the drying column in the production of toluenedia- (T) mine via hydrogenation of dinitrotoluene.

Condensed liquid light ends from the purification of toluenediamine in the production (T) of toluenediamine via hydrogenation of dinitrotoluene.

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Vicinals from the purification of toluenediamine in the production of toluenediamine (T) via hydrogenation of dinitrotoluene.

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Heavy ends from the purification of toluenediamine in the production of toluenedia- | (T) mine via hydrogenation of dinitrotoluene.

Organic condensate from the solvent recovery column in the production of toluene (T) diisocyanate via phosgenation of toluenediamine.

Wastewater from the reactor vent gas scrubber in the production of ethylene (T) dibromide via bromination of ethene.

Spent adsorbent solids from purification of ethylene dibromide in the production of (T) ethylene dibromide via bromination of ethene.

Still bottoms from the purification of ethylene dibromide in the production of ethylene (T) dibromide via bromination of ethene.

Brine purification muds from the mercury cell process in chlorine production, where (T) separately prepurified brine is not used.

Chlorinated hydrocarbon waste from the purification step of the diaphragm cell (T) process using graphite anodes in chlorine production.

Wastewater treatment sludge from the mercury cell process in chlorine production...

By-product salts generated in the production of MSMA and cacodylic acid.
Wastewater treatment sludge from the production of chlordane....

(T)

Wastewater and scrub water from the chlorination of cyclopentadiene in the (T) production of chlordane.

Filter solids from the filtration of hexachlorocyclopentadiene in the production of (T) chlordane.

Wastewater treatment sludges generated in the production of creosote....

Still bottoms from toluene reclamation distillation in the production of disulfoton.
Wastewater treatment sludges from the production of disulfoton..
Wastewater from the washing and stripping of phorate production..

Filter cake from the filtration of diethylphosphorodithioic acid in the production of
phorate.

Wastewater treatment sludge from the production of phorate
Wastewater treatment sludge from the production of toxaphene

Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the
production of 2,4,5-T.

2,6-Dichlorophenol waste from the production of 2,4-D

(T)

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Vacuum stripper discharge from the chlordane chlorinator in the production of (T)
chlordane.

Untreated process wastewater from the production of toxaphene
Untreated wastewater from the production of 2,4-D.

Process wastewater (including supernates, filtrates, and washwaters) from the (T)
production of ethylenebisdithiocarbamic acid and its salt.

Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid (C, T)
and its salts.
Filtration, evaporation, and centrifugation solids from the production of ethylenebis- (T)
dithiocarbamic acid and its salts.

Baghouse dust and floor sweepings in milling and packaging operations from the (T)
production or formulation of ethylenebisdithiocarbamic acid and its salts.

Wastewater from the reactor and spent sulfuric acid from the acid dryer from the (C, T) production of methyl bromide.

Spent absorbent and wastewater separator solids from the production of methyl (T) bromide.

Explosives:

K044

K045

K046

K047

Petroleum refining:

K048

K049

K050

K051

K052

Iron and steel:

K061

K062

Primary copper:
K064

Wastewater treatment sludges from the manufacturing and processing of explosives... (R)
Spent carbon from the treatment of wastewater containing explosives....

Wastewater treatment sludges from the manufacturing, formulation and loading of❘ (T) lead-based initiating compounds.

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Emission control dust/sludge from the primary production of steel in electric (T) furnaces.

Spent pickle liquor generated by steel finishing operations of facilities within the iron (C,T) and steel industry (SIC Codes 331 and 332).

Acid plant blowdown slurry/sludge resulting from the thickening of blowdown slurry (T) from primary copper production.

Industry and EPA hazardous waste No.

Primary lead:

K065

Primary zinc: K066

Primary aluminum: K088 Ferroalloys

K090 K091

Secondary lead: K069....

K100

Veterinary pharmaceuticals: K084

K101

K102

Ink formulation: K086

Coking: K060 K087

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Surface impoundment solids contained in and dredged from surface impoundments (T) at primary lead smelting facilities

Sludge from treatment of process wastewater and/or acid plant blowdown from (T) primary zinc production.

Spent potliners from primary aluminum reduction

Emission control dust or sludge from ferrochromiumsilicon production
Emission control dust or sludge from ferrochromium production

(T)

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Emission control dust/sludge from secondary lead smelting. (NOTE: This listing is (T)
stayed administratively for sludge generated from secondary acid scrubber sys-
tems. The stay will remain in effect until further administrative action is taken if !
EPA takes further action effecting this stay, EPA will publish a notice of the action!
in the Federal Register.

Waste leaching solution from acid leaching of emission control dust/sludge from (T)
secondary lead smelting.

Wastewater treatment sludges generated during the production of veterinary pharma- (T) ceuticals from arsenic or organo-arsenic compounds.

Distillation tar residues from the distillation of aniline-based compounds in the (T) production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.

Residue from the use of activated carbon for decolorization in the production of (T) veterinary pharmaceuticals from arsenic or organo-arsenic compounds.

Solvent washes and sludges, caustic washes and sludges, or water washes and (T) sludges from cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and stabilizers containing chromium and lead.

Ammonia still lime sludge from coking operations..
Decanter tank tar sludge from coking operations.

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[46 FR 4618, Jan. 16, 1981]

EDITORIAL NOTE: For Federal RegiSTER citations affecting § 261.32, see the List of CFR Sections Affected in the Finding Aids section of this volume.

§ 261.33 Discarded commercial chemical

products, off-specification species, container residues, and spill residues thereof.

The following materials or items are hazardous wastes if and when they are discarded or intended to be discarded as described in § 261.2(a)(2)(i), when they are mixed with waste oil or used oil or other material and applied to the land for dust suppression or road treatment, when they are otherwise applied to the land in lieu of their original intended use or when they are contained in products that are applied to the land in lieu of their original intended use, or when, in lieu of their original intended use, they are produced for use as (or as a component of) a fuel, distributed for use as a fuel, or burned as a fuel.

(a) Any commercial chemical product, or manufacturing chemical inter

mediate having the generic name listed in paragraph (e) or (f) of this section.

(b) Any off-specification commercial chemical product or manufacturing chemical intermediate which, if it met specifications, would have the generic name listed in paragraph (e) or (f) of this section.

(c) Any residue remaining in a container or in an inner liner removed from a container that has held any commercial chemical product or manufacturing chemical intermediate having the generic name listed in paragraphs (e) or (f) of this section, unless the container is empty as defined in § 261.7(b) of this chapter.

[Comment: Unless the residue is being beneficially used or reused, or legitimately recycled or reclaimed; or being accumulated, stored, transported or treated prior to such use, re-use, recycling or reclamation, EPA

considers the residue to be intended for discard, and thus, a hazardous waste. An example of a legitimate re-use of the residue would be where the residue remains in the container and the container is used to hold the same commercial chemical product or manufacturing chemical intermediate it previously held. An example of the discard of the residue would be where the drum is sent to a drum reconditioner who reconditions the drum but discards the residue.]

(d) Any residue or contaminated soil, water or other debris resulting from the cleanup of a spill into or on any land or water of any commercial chemical product or manufacturing chemical intermediate having the generic name listed in paragraph (e) or (f) of this section, or any residue or contaminated soil, water or other debris resulting from the cleanup of a spill, into or on any land or water, of any off-specification chemical product and manufacturing chemical intermediate which, if it met specifications, would have the generic name listed in paragraph (e) or (f) of this section.

[Comment: The phrase "commercial chemical product or manufacturing chemical intermediate having the generic name listed in..." refers to a chemical substance which is manufactured or formulated for commercial or manufacturing use which consists of the commercially pure grade of

the chemical, any technical grades of the chemical that are produced or marketed, and all formulations in which the chemical is the sole active ingredient. It does not refer to a material, such as a manufacturing process waste, that contains any of the substances listed in paragraph (e) or (f). Where a manufacturing process waste is deemed to be a hazardous waste because it contains a substance listed in paragraph (e) or (f), such waste will be listed in either § 261.31 or § 261.32 or will be identified as a hazardous waste by the characteristics set forth in subpart C of this part.]

(e) The commercial chemical products, manufacturing chemical intermediates or off-specification commercial chemical products or manufacturing chemical intermediates referred to in paragraphs (a) through (d) of this section, are identified as acute hazardous wastes (H) and are subject to be the small quantity exclusion defined in § 261.5(e).

[Comment: For the convenience of the regulated community the primary hazardous properties of these materials have been indicated by the letters T (Toxicity), and R (Reactivity). Absence of a letter indicates that the compound only is listed for acute toxicity.]

These wastes and their corresponding EPA Hazardous Waste Numbers

are:

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311-147 0-92--3

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