Circular of the National Bureau of Standards, Issue 440U.S. Government Printing Office, 1942 |
From inside the book
Results 1-5 of 100
Page 81
... SOLUTION The rotation of the normal sugar solution for λ = 5461 A was found by direct measurement . Normal sugar solution = 100 ° sugar = 40.763 ° . ( 21 ) Since the rotation ratio for the normal solution for λ = 5892.5 A and λ = 5461 A ...
... SOLUTION The rotation of the normal sugar solution for λ = 5461 A was found by direct measurement . Normal sugar solution = 100 ° sugar = 40.763 ° . ( 21 ) Since the rotation ratio for the normal solution for λ = 5892.5 A and λ = 5461 A ...
Page 85
... solution of sugar the rotatory dispersion is nearly the same as that of quartz , but the divergence is sufficient in the green and blue end of the spectrum ( see fig . 19 curves S , Q , and S - Q ) to cause the halves of the field to ...
... solution of sugar the rotatory dispersion is nearly the same as that of quartz , but the divergence is sufficient in the green and blue end of the spectrum ( see fig . 19 curves S , Q , and S - Q ) to cause the halves of the field to ...
Page 120
... solution . In 1909 The International Commission for Uniform Methods of Sugar Analysis , adopted the solution of basic lead acetate of the German Pharmacopoeia , which is prepared by boiling 3 parts normal lead acetate , 1 part lead ...
... solution . In 1909 The International Commission for Uniform Methods of Sugar Analysis , adopted the solution of basic lead acetate of the German Pharmacopoeia , which is prepared by boiling 3 parts normal lead acetate , 1 part lead ...
Page 120
... solution should be used . This quantity is gaged with requisite accuracy by experienced workers . The needed quantities for particular cases cannot be stated , but the following approximate numbers are given as examples : For Java ...
... solution should be used . This quantity is gaged with requisite accuracy by experienced workers . The needed quantities for particular cases cannot be stated , but the following approximate numbers are given as examples : For Java ...
Page 120
... solution . The result in either case is an increase in dextrorotation or a higher polarization . Prinsen Geerligs has shown that basic acetate of lead precipitates levulose when the same solution contains salts which are capable of ...
... solution . The result in either case is an increase in dextrorotation or a higher polarization . Prinsen Geerligs has shown that basic acetate of lead precipitates levulose when the same solution contains salts which are capable of ...
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Common terms and phrases
alkaline analysis angle axis beam boiling Brix Bureau of Standards C. S. Hudson calculated carbon cell CHCl3 Chem chloride Clerget coefficient color concentration constant containing cooled copper correction crystals determined deut dextrose dilute direct polarization dissolved electrode equation evaporated filter filtrate flask formula glass glycosides grams H. S. Isbell H₂O halfshade heating hydrochloric acid hydrolysis instrument invert sugar invertase Jackson and Gillis lactose lamp lead acetate levulose measurements melting method methyl alcohol mg mg mg mixture molasses mutarotation nicol nicol prism normal weight obtained optical rotation oscillation oxide percent percentage plane polarized polariscope polarized light potassium precipitate prepared prism quantity quartz quartz control plates raffinose reaction reading reagent reducing sugars refracting saccharimeter salts sample sirup sodium specific rotation substance sucrose sucrose solutions Sugar Scale sugar solution sulfate sulfuric acid temperature tion titration tube vacuo volume washed wave length
Popular passages
Page 158 - If the analyst is in doubt as to the completion of the hydrolysis, allow a portion of the solution to remain for several hours and again polarize. If there is no change from the previous reading, the inversion is complete, and the reading and temperature of the solution should be carefully noted.
Page 181 - Titrate at once with the thiosulphate solution until the brown tinge has become weak, then add sufficient starch liquor to produce a marked blue coloration. Continue the titration cautiously until the color due to free iodin has entirely vanished.
Page 778 - After bringing the solution exactly to the mark at the proper temperature, and after wiping out the neck of the flask with filter paper, pour all of the wellshaken clarified sugar solution on a rapidly acting filter. Reject the first portions of the filtrate and use the rest, which must be perfectly clear for polarization.
Page 250 - In case the sample is too dense to determine the density directly, dilute a weighed portion with a weighed quantity of water, or dissolve a weighed portion and dilute to a known volume with water. In the first instance the per cent of total solids is calculated by the following formula : • WS Per cent of solids in the undiluted material= — • S=per cent of solids in the diluted material.
Page 789 - Receptacles — How sampled. — Sugar in hogsheads and other wooden packages shall be sampled by putting the long trier diagonally through the package from chime to chime, one trierful to constitute a sample, except in small lots, when an equal number of trierfuls shall be taken from each package to furnish the required amount of sugar necessary to make a sufficient sample. In the sampling of baskets, bags, seroons, and mats the short trier shall be used, care being exercised to have each sample...
Page 120 - Add strong ammonium hydroxide with constant stirring until the solution is alkaline to litmus, allow the precipitate to settle, and wash by decantation with water until the wash water gives only a slight test for sulfates with barium chloride solution.
Page 170 - Alkaline tartrate solution. — Dissolve 173 g of Rochelle salt and 50 g of sodium hydroxide in water, and dilute to 500 ml.
Page 155 - Defecate, if necessary, with basic lead acetate in the usual manner, making to volume at the temperature at which the observations are to be made.
Page 177 - By consulting the table it will be seen that the vertical column headed 150 is nearest to Z, 145, and the horizontal column headed 95 : 5 is nearest to the ratio of R to I, 95.1 : 4.9.
Page 783 - Inasmuch as the absorption of sea water or moisture reduces the polariscopic test of sugar, there shall be no allowance on account of increased weight of sugar importations due to unusual absorption of sea water or other moisture while on the voyage of importation.