Circular of the National Bureau of Standards, Issue 440U.S. Government Printing Office, 1942 |
From inside the book
Results 1-5 of 99
Page v
... baths . 110 5. Weights --- 110 ( a ) Sugar .. 110 ( b ) Analytical_ ( c ) Reference standards .. ( d ) Certification___ 111 111 111 ( e ) Submission of weights for test . 6. Balances .. 7. References . 112 112 113 PART 2. - RAW AND ...
... baths . 110 5. Weights --- 110 ( a ) Sugar .. 110 ( b ) Analytical_ ( c ) Reference standards .. ( d ) Certification___ 111 111 111 ( e ) Submission of weights for test . 6. Balances .. 7. References . 112 112 113 PART 2. - RAW AND ...
Page x
... bath . 3. Procedure ... ( a ) Equilibrium water . 267 268 268 269 270 271 271 ( b ) Preparation of potassium chloride solution :. ( c ) Determination of cell constants .. ( d ) Checking of cells ... 4. Specific conductance of solutions ...
... bath . 3. Procedure ... ( a ) Equilibrium water . 267 268 268 269 270 271 271 ( b ) Preparation of potassium chloride solution :. ( c ) Determination of cell constants .. ( d ) Checking of cells ... 4. Specific conductance of solutions ...
Page 46
... bath . An electric heater then brings the bath temperature up to the proper point and maintains it there . The heater is made of fine resistance wire wound around a large framework which fits inside the box . See figs . 26 and 27 , p ...
... bath . An electric heater then brings the bath temperature up to the proper point and maintains it there . The heater is made of fine resistance wire wound around a large framework which fits inside the box . See figs . 26 and 27 , p ...
Page 61
... bath of the circular - scale polariscope described on page 46 , and the optical rotation carefully measured at 20 ° C for spectrally purified mercury light of wave length 5461 A. In order to eliminate accidental errors as far as ...
... bath of the circular - scale polariscope described on page 46 , and the optical rotation carefully measured at 20 ° C for spectrally purified mercury light of wave length 5461 A. In order to eliminate accidental errors as far as ...
Page 90
... a source for photomicrographic work. FIGURE 22. - White - light sources . FIGURE 26. Inside view of polariscope air bath ( thermostated. 90 Circular of the National Bureau of Standards (1) Monochromatic_ (2) White light.
... a source for photomicrographic work. FIGURE 22. - White - light sources . FIGURE 26. Inside view of polariscope air bath ( thermostated. 90 Circular of the National Bureau of Standards (1) Monochromatic_ (2) White light.
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Common terms and phrases
alkaline analysis angle axis beam boiling Brix Bureau of Standards C. S. Hudson calculated carbon cell CHCl3 Chem chloride Clerget coefficient color concentration constant containing cooled copper correction crystals determined deut dextrose dilute direct polarization dissolved electrode equation evaporated filter filtrate flask formula glass glycosides grams H. S. Isbell H₂O halfshade heating hydrochloric acid hydrolysis instrument invert sugar invertase Jackson and Gillis lactose lamp lead acetate levulose measurements melting method methyl alcohol mg mg mg mixture molasses mutarotation nicol nicol prism normal weight obtained optical rotation oscillation oxide percent percentage plane polarized polariscope polarized light potassium precipitate prepared prism quantity quartz quartz control plates raffinose reaction reading reagent reducing sugars refracting saccharimeter salts sample sirup sodium specific rotation substance sucrose sucrose solutions Sugar Scale sugar solution sulfate sulfuric acid temperature tion titration tube vacuo volume washed wave length
Popular passages
Page 158 - If the analyst is in doubt as to the completion of the hydrolysis, allow a portion of the solution to remain for several hours and again polarize. If there is no change from the previous reading, the inversion is complete, and the reading and temperature of the solution should be carefully noted.
Page 181 - Titrate at once with the thiosulphate solution until the brown tinge has become weak, then add sufficient starch liquor to produce a marked blue coloration. Continue the titration cautiously until the color due to free iodin has entirely vanished.
Page 778 - After bringing the solution exactly to the mark at the proper temperature, and after wiping out the neck of the flask with filter paper, pour all of the wellshaken clarified sugar solution on a rapidly acting filter. Reject the first portions of the filtrate and use the rest, which must be perfectly clear for polarization.
Page 250 - In case the sample is too dense to determine the density directly, dilute a weighed portion with a weighed quantity of water, or dissolve a weighed portion and dilute to a known volume with water. In the first instance the per cent of total solids is calculated by the following formula : • WS Per cent of solids in the undiluted material= — • S=per cent of solids in the diluted material.
Page 789 - Receptacles — How sampled. — Sugar in hogsheads and other wooden packages shall be sampled by putting the long trier diagonally through the package from chime to chime, one trierful to constitute a sample, except in small lots, when an equal number of trierfuls shall be taken from each package to furnish the required amount of sugar necessary to make a sufficient sample. In the sampling of baskets, bags, seroons, and mats the short trier shall be used, care being exercised to have each sample...
Page 120 - Add strong ammonium hydroxide with constant stirring until the solution is alkaline to litmus, allow the precipitate to settle, and wash by decantation with water until the wash water gives only a slight test for sulfates with barium chloride solution.
Page 170 - Alkaline tartrate solution. — Dissolve 173 g of Rochelle salt and 50 g of sodium hydroxide in water, and dilute to 500 ml.
Page 155 - Defecate, if necessary, with basic lead acetate in the usual manner, making to volume at the temperature at which the observations are to be made.
Page 177 - By consulting the table it will be seen that the vertical column headed 150 is nearest to Z, 145, and the horizontal column headed 95 : 5 is nearest to the ratio of R to I, 95.1 : 4.9.
Page 783 - Inasmuch as the absorption of sea water or moisture reduces the polariscopic test of sugar, there shall be no allowance on account of increased weight of sugar importations due to unusual absorption of sea water or other moisture while on the voyage of importation.