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Petroleum refinery primary oil/water/solids separation sludge-Any sludge generated from the gravitational separation of oil/water/solids during the storage or treatment of process wastewaters from petroleum refineries. Such sludges include, but are not limited to, those generated in: oil/water/solids separators; tanks and impoundments; ditches and other conveyances; sumps; and stormwater units receiving dry weather flow. Sludge generated in stormwater units that do not receive dry weather flow, sludges generated from non-contact once-through cooling waters segregated for treatment from other process or oily cooling waters, sludges generated in aggressive biological treatment units as defined in §261.31(b)(2) (including sludges generated in one or more additional units after wastewaters have been treated in aggressive biological treatment units) and K051 Hwastes are not included in this listing.

Petroleum refinery secondary (emulsified) oil/water/solids separation sludge Any sludge and/or float generated from the physical and/or chemical separation of oil/water/solids in process wastewaters and oily cooling wastewaters from petroleum refineries. Such wastes include, but are not limited to, all sludges and floats generated in: induced air flotation (IAF) units, tanks and impoundments, and all sludges generated in DAF units. Sludges generated in stormwater units that do not receive dry weather flow, sludges generated from Konce-through non-contact cooling waters segregated for treatment from other process or oil cooling wastes, sludges and floats generated in aggressive biological treatment units as defined in $261.31(b)(2) (including sludges and floats generated in one or more additional units after wastewaters have been treated in aggressive biological treatment units) and F037, K048, and K051 wastes are not included in this listing.

K001

Bottom sediment sludge from the treatment of wastewaters from wood
preserving processes that use creosote and/or pentachlorophenol.
K002 O

Wastewater treatment sludge from the production of chrome yellow and
orange pigments.

K003

Wastewater treatment sludge from the production of molybdate orange
pigments.

K004

Wastewater treatment sludge from the production of zinc yellow pig

ments.

K005

Wastewater treatment sludge from the production of chrome green pig-
ments.

K006

Wastewater treatment sludge from the production of chrome oxide green pigments (anhydrous and hydrated).

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TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-Continued [Note: All Comments/Notes Are Located at the End of This Table]

K007

Hazardous substance

Wastewater treatment sludge from the production of iron blue pigments.

K008

Oven residue from the production of chrome oxide green pigments.
K009

Distillation bottoms from the production of acetaldehyde from ethylene.
K010

Distillation side cuts from the production of acetaldehyde from ethylene.
K011

Bottom stream from the wastewater stripper in the production of acrylo-
nitrile.

K013

Bottom stream from the acetonitrile column in the production of acrylo-
nitrile.

K014

Bottoms from the acetonitrile purification column in the production of acrylonitrile.

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Heavy ends or distillation residues from the production of carbon tetrachloride.

K017

Heavy ends (still bottoms) from the purification column in the production
of epi-chlorohydrin.

K018

Heavy ends from the fractionation column in ethyl chloride production.
K019

Heavy ends from the distillation of ethylene dichloride in ethylene dichlo-
ride production.

K020

Heavy ends from the distillation of vinyl chloride in vinyl chloride mon-
omer production.

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Distillation bottom tars from the production of phenol/acetone from cumene.

K023

Distillation light ends from the production of phthalic anhydride from naphthalene.

K024

Distillation bottoms from the production of phthalic anhydride from naphthalene.

K025

Distillation bottoms from the production of nitrobenzene by the nitration
of benzene.

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Centrifuge and distillation residues from toluene diisocyanate production. K028

Spent catalyst from the hydrochlorinator reactor in the production of 1,1,1-trichloroethane.

K029

Waste from the product steam stripper in the production of 1,1,1-trichloroethane.

K030

Column bottoms or heavy ends from the combined production of tri-
chloroethylene and perchloroethylene.

K031

By-product salts generated in the production of MSMA and cacodylic

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Wastewater treatment sludge from the production of chlordane. K033

Wastewater and scrub water from the chlorination of cyclopentadiene in the production of chlordane.

K034

Filter solids from the filtration of hexachlorocyclopentadiene in the pro-
duction of chlordane.

K035

Wastewater treatment sludges generated in the production of creosote.

K036

Still bottoms from toluene reclamation distillation in the production of
disulfoton.

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TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-Continued [Note: All Comments/Notes Are Located at the End of This Table]

Hazardous substance

CASRN

Filter cake from the filtration of diethylphosphorodithioic acid in the production of phorate.

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4❘ K041

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K041

Wastewater treatment sludge from the production of toxaphene.

K042

Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production of 2,4,5-T.

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Wastewater treatment sludges from the manufacturing and processing of explosives.

K045

Spent carbon from the treatment of wastewater containing explosives.
K046

Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based initiating compounds.

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Dissolved air flotation (DAF) float from the petroleum refining industry.

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Heat exchanger bundle cleaning sludge from the petroleum refining industry.

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Emission control dust/sludge from the primary production of steel in

electric furnaces.

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K062

Spent pickle liquor generated by steel finishing operations of factilties within the iron and steel industry (SIC Codes 331 and 332).

K064

Acid plant blowdown slurry/sludge resulting from thickening of blowdown slurry from primary copper production.

K065

Surface impoundment solids contained in and dredged from surface impoundments at primary lead smelting facilities.

K066

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Sludge from treatment of process wastewater and/or acid plant blowdown from primary zinc production.

4 K073

1 (0.454)

10 (4.54)

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Brine purification muds from the mercury cell process in chlorine pro-
duction, where separately prepurified brine is not used.

K073

Chlorinated hydrocarbon waste from the purification step of the dia-
phragm cell process using graphite anodes in chlorine production.
K083

Distillation bottoms from aniline extraction.
K084

Wastewater treatment sludges generated during the production of vet-
erinary pharmaceuticals from arsenic or organo-arsenic compounds.
K085

Distillation or fractionation column bottoms from the production of
chlorobenzenes.

K086

Solvent washes and sludges, caustic washes and sludges, or water
washes and sludges from cleaning tubs and equipment used in the
formulation of ink from pigments, driers, soaps, and stabilizers con-
taining chromium and lead.

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Distillation light ends from the production of phthalic anhydride from ortho-xylene.

K094

4 K087

100 (45.4)

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